The GCMS Analysis of Volatile Components Extracted by Different Methods from Exocarpium Citri Grandis
Joint Authors
Xie, Zhisheng
Yang, Depo
Liu, Qundi
Liang, Zhikun
Xu, Xin-jun
Zhao, Mingqian
Yu, Xiaoxue
Source
Journal of Analytical Methods in Chemistry
Issue
Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-8, 8 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2013-11-17
Country of Publication
Egypt
No. of Pages
8
Main Subjects
Abstract EN
Volatile components from Exocarpium Citri Grandis (ECG) were, respectively, extracted by three methods, that is, steam distillation (SD), headspace solid-phase microextraction (HS-SPME), and solvent extraction (SE).
A total of 81 compounds were identified by gas chromatography-mass spectrometry including 77 (SD), 56 (HS-SPME), and 48 (SE) compounds, respectively.
Despite of the extraction method, terpenes (39.98~57.81%) were the main volatile components of ECG, mainly germacrene-D, limonene, 2,6,8,10,14-hexadecapentaene, 2,6,11,15-tetramethyl-, (E,E,E)-, and trans-caryophyllene.
Comparison was made among the three methods in terms of extraction profile and property.
SD relatively gave an entire profile of volatile in ECG by long-time extraction; SE enabled the analysis of low volatility and high molecular weight compounds but lost some volatiles components; HS-SPME generated satisfactory extraction efficiency and gave similar results to those of SD at analytical level when consuming less sample amount, shorter extraction time, and simpler procedure.
Although SD and SE were treated as traditionally preparative extractive techniques for volatiles in both small batches and large scale, HS-SPME coupled with GC/MS could be useful and appropriative for the rapid extraction and qualitative analysis of volatile components from medicinal plants at analytical level.
American Psychological Association (APA)
Xie, Zhisheng& Liu, Qundi& Liang, Zhikun& Zhao, Mingqian& Yu, Xiaoxue& Yang, Depo…[et al.]. 2013. The GCMS Analysis of Volatile Components Extracted by Different Methods from Exocarpium Citri Grandis. Journal of Analytical Methods in Chemistry،Vol. 2013, no. 2013, pp.1-8.
https://search.emarefa.net/detail/BIM-508074
Modern Language Association (MLA)
Xie, Zhisheng…[et al.]. The GCMS Analysis of Volatile Components Extracted by Different Methods from Exocarpium Citri Grandis. Journal of Analytical Methods in Chemistry No. 2013 (2013), pp.1-8.
https://search.emarefa.net/detail/BIM-508074
American Medical Association (AMA)
Xie, Zhisheng& Liu, Qundi& Liang, Zhikun& Zhao, Mingqian& Yu, Xiaoxue& Yang, Depo…[et al.]. The GCMS Analysis of Volatile Components Extracted by Different Methods from Exocarpium Citri Grandis. Journal of Analytical Methods in Chemistry. 2013. Vol. 2013, no. 2013, pp.1-8.
https://search.emarefa.net/detail/BIM-508074
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-508074