Sol-Gel Synthesis and Characterization of Ag3(2+x)AlxTi4−xO11+δ (0.0≤ x ≤1.0) Nanoparticles
Author
Source
Issue
Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-8, 8 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2013-08-22
Country of Publication
Egypt
No. of Pages
8
Main Subjects
Engineering Sciences and Information Technology
Chemistry
Abstract EN
The Ag3(2+x)AlxTi4−xO11+δ (0.0≤x≤1.0; B1–B5) nanoparticles have been synthesized by sol-gel technique.
X-ray diffraction, scanning electron microscopy, optical absorption spectroscopy, and electron paramagnetic resonance spectroscopy were used to characterize the sample.
The X-ray diffraction results indicate the formation of nanocrystalline materials in tetragonal lattice with P42/nnm space group.
The identical distribution of elements were confirmed by scanning electron microscopy with energy dispersive X-ray spectrometry and X-ray mapping.
Electron paramagnetic resonance lineshapes of the samples are obtained at various (13 K, 77 K, and 300 K) temperatures.
The isotropic lineshapes of the sample B1 are attributed to dipole-dipole interaction of Ti3+ ions.
The incorporation of Al3+ ions into the sample B2–B5 the isotropic nature of the lineshapes are collapsed due to the distraction in crystal field.
Optical absorption spectra results reveal the presence of Ag-TiO2 nanoparticles.
American Psychological Association (APA)
Ramesh, S.. 2013. Sol-Gel Synthesis and Characterization of Ag3(2+x)AlxTi4−xO11+δ (0.0≤ x ≤1.0) Nanoparticles. Journal of Nanoscience،Vol. 2013, no. 2013, pp.1-8.
https://search.emarefa.net/detail/BIM-508975
Modern Language Association (MLA)
Ramesh, S.. Sol-Gel Synthesis and Characterization of Ag3(2+x)AlxTi4−xO11+δ (0.0≤ x ≤1.0) Nanoparticles. Journal of Nanoscience No. 2013 (2013), pp.1-8.
https://search.emarefa.net/detail/BIM-508975
American Medical Association (AMA)
Ramesh, S.. Sol-Gel Synthesis and Characterization of Ag3(2+x)AlxTi4−xO11+δ (0.0≤ x ≤1.0) Nanoparticles. Journal of Nanoscience. 2013. Vol. 2013, no. 2013, pp.1-8.
https://search.emarefa.net/detail/BIM-508975
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-508975