Synthesis and Crystal Structure of 2-(Dichloromethyl)‎-2-(4-nitrophenyl)‎-1,3-dioxane

Joint Authors

Ye, Fei
Sun, Chang-Ying
Fu, Ying

Source

Journal of Chemistry

Issue

Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-4, 4 p.

Publisher

Hindawi Publishing Corporation

Publication Date

2013-11-24

Country of Publication

Egypt

No. of Pages

4

Main Subjects

Chemistry

Abstract EN

A new compound, 2-dichloromethyl-2-p-nitrophenyl-1,3-dioxane, was synthesized and characterized.

The crystal structure of the title compound (C11H11Cl2NO4, Mr=292.11) has been determined by single-crystal X-ray diffraction.

The crystal is of monoclinic, space group P21/c with a=11.013(2) Å, b=14.653(3) Å, c=7.8693(16) Å, α=90°, β=97.06(3)°, γ=90°, V=1260.3(4) Å3, Z=4, F(000)=600, Dc=1.540 mg/cm3, the final R1=0.0508, and ωR2=0.1072 for observed reflections with I>2σI.

A total of 12162 reflections were collected, of which 2867 were unique (Rint=0.06999).

American Psychological Association (APA)

Ye, Fei& Sun, Chang-Ying& Fu, Ying. 2013. Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane. Journal of Chemistry،Vol. 2013, no. 2013, pp.1-4.
https://search.emarefa.net/detail/BIM-512741

Modern Language Association (MLA)

Ye, Fei…[et al.]. Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane. Journal of Chemistry No. 2013 (2013), pp.1-4.
https://search.emarefa.net/detail/BIM-512741

American Medical Association (AMA)

Ye, Fei& Sun, Chang-Ying& Fu, Ying. Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane. Journal of Chemistry. 2013. Vol. 2013, no. 2013, pp.1-4.
https://search.emarefa.net/detail/BIM-512741

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references

Record ID

BIM-512741