Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane
Joint Authors
Ye, Fei
Sun, Chang-Ying
Fu, Ying
Source
Issue
Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-4, 4 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2013-11-24
Country of Publication
Egypt
No. of Pages
4
Main Subjects
Abstract EN
A new compound, 2-dichloromethyl-2-p-nitrophenyl-1,3-dioxane, was synthesized and characterized.
The crystal structure of the title compound (C11H11Cl2NO4, Mr=292.11) has been determined by single-crystal X-ray diffraction.
The crystal is of monoclinic, space group P21/c with a=11.013(2) Å, b=14.653(3) Å, c=7.8693(16) Å, α=90°, β=97.06(3)°, γ=90°, V=1260.3(4) Å3, Z=4, F(000)=600, Dc=1.540 mg/cm3, the final R1=0.0508, and ωR2=0.1072 for observed reflections with I>2σI.
A total of 12162 reflections were collected, of which 2867 were unique (Rint=0.06999).
American Psychological Association (APA)
Ye, Fei& Sun, Chang-Ying& Fu, Ying. 2013. Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane. Journal of Chemistry،Vol. 2013, no. 2013, pp.1-4.
https://search.emarefa.net/detail/BIM-512741
Modern Language Association (MLA)
Ye, Fei…[et al.]. Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane. Journal of Chemistry No. 2013 (2013), pp.1-4.
https://search.emarefa.net/detail/BIM-512741
American Medical Association (AMA)
Ye, Fei& Sun, Chang-Ying& Fu, Ying. Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane. Journal of Chemistry. 2013. Vol. 2013, no. 2013, pp.1-4.
https://search.emarefa.net/detail/BIM-512741
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-512741