Separation and identification of hydrocarbons and other volatile compounds from cultures of Aspergillus niger by GC–MS using two different capillary columns and solvents
Joint Authors
Siddiqi, Shafiquzzaman
al-Azad, Sujjat
Abu Bakar, Fatimah
Nahir, Layla
Kumar, S. Vijay
Source
Journal of Saudi Chemical Society
Issue
Vol. 19, Issue 3 (30 Jun. 2015), pp.243-256, 14 p.
Publisher
Publication Date
2015-06-30
Country of Publication
Saudi Arabia
No. of Pages
14
Main Subjects
Topics
Abstract EN
A simple, fast, repeatable, and less laborious sample-preparation protocol based on gas chromatography–mass spectrometry was developed and applied for the analysis of bioactive compounds derived from the filamentous fungus Aspergillus niger strain SS10.
The match factors for the spectra of the samples with reference to the mass-spectral library of fungal volatile compounds were determined and used to study the complex hydrocarbons and other volatile compounds that were separated using two different capillary columns and nonpolar and medium-polar stationary phases.
More than 295 volatile compounds (spectral match factor of at least 90 %), such as normal saturated hydrocarbons (C7–C30), cyclohexane, cyclopentane, fatty acids, alcohols, esters, sulfur- and bromo-containing compounds, simple pyrane, and benzene derivatives, were identified.
Most of these compounds have not been reported earlier.
The method described in this article is a suitable research tool for the determination of volatile compounds from the cultures of A.
niger.
American Psychological Association (APA)
Siddiqi, Shafiquzzaman& al-Azad, Sujjat& Abu Bakar, Fatimah& Nahir, Layla& Kumar, S. Vijay. 2015. Separation and identification of hydrocarbons and other volatile compounds from cultures of Aspergillus niger by GC–MS using two different capillary columns and solvents. Journal of Saudi Chemical Society،Vol. 19, no. 3, pp.243-256.
https://search.emarefa.net/detail/BIM-566109
Modern Language Association (MLA)
Siddiqi, Shafiquzzaman…[et al.]. Separation and identification of hydrocarbons and other volatile compounds from cultures of Aspergillus niger by GC–MS using two different capillary columns and solvents. Journal of Saudi Chemical Society Vol. 19, no. 3 (2015), pp.243-256.
https://search.emarefa.net/detail/BIM-566109
American Medical Association (AMA)
Siddiqi, Shafiquzzaman& al-Azad, Sujjat& Abu Bakar, Fatimah& Nahir, Layla& Kumar, S. Vijay. Separation and identification of hydrocarbons and other volatile compounds from cultures of Aspergillus niger by GC–MS using two different capillary columns and solvents. Journal of Saudi Chemical Society. 2015. Vol. 19, no. 3, pp.243-256.
https://search.emarefa.net/detail/BIM-566109
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 255-256
Record ID
BIM-566109