Preparation and characterization of yttrium oxide nanoparticles at different calcination temperatures from yttrium hydroxide prepared by hydrothermal and hydrothermal microwave methods

Other Title(s)

تحضير و تشخيص دقائق أوكسيد الاتريوم النانوية في درجات حرارة تلدين مختلفة من هيدروكسيد الاتريوم المحضر بطريقتي الھيدروحرارية و الھيدروحرارية-الموجات الدقيقة

Joint Authors

al-Ukaydi, Walid Mazlum
Abd al-Ghani, Ahlam Jamil

Source

Iraqi Journal of Science

Issue

Vol. 56, Issue 2C (30 Sep. 2015), pp.1572-1587, 16 p.

Publisher

University of Baghdad College of Science

Publication Date

2015-09-30

Country of Publication

Iraq

No. of Pages

16

Main Subjects

Chemistry

Abstract AR

تم تحضير دقائق اوكسيد الاتريوم النانوية من تسخين ھيدروكسيد الاتريوم المحضر من نترات االتريوم مع ھيدروكسيد الصوديوم في الدالة الحامضية 13 باستخدام طريقتي الھيدرو حراري الاعتيادي و الھيدرو حراري باستخدام أشعة الموجات الدقيقة.

تمت دراسة تأثير المعاملة الحرارية للھيدروكسيد الناتج على الھيئة البلورية و أشكال مسحوق الاوكسيد النانوي الناتج في درجات التلدين 500 و700 و1000◦ م.

شخصت النواتج باعتماد تحاليل حيود الأشعة السينية و المجھر الالكتروني الماسح و مجھر القوة الذرية و مطيافية الأشعة تحت الحمراء و التحاليل الحرارية.

Abstract EN

The Synthesis of yttrium oxide nanoparticles have been achieved via calcination of yttrium hydroxide produced from the reaction of aqueous solutions of yttrium nitrate and sodium hydroxide at pH = 13 using hydrothermal and hydrothermal microwave methods.

Effect of heat treatment of the resulted yttrium hydroxide powder on the morphology and crystallinity of the resulting oxide was studied at calcination 500, 700 and 1000°C to obtain.

The resulted products were characterized by means of X-ray diffraction (XRD), scanning electron microscope (SEM), atomic force microscope (AFM), Fourier transform infrared spectrometer (FTIR) and thermal analyses (TG).

American Psychological Association (APA)

Abd al-Ghani, Ahlam Jamil& al-Ukaydi, Walid Mazlum. 2015. Preparation and characterization of yttrium oxide nanoparticles at different calcination temperatures from yttrium hydroxide prepared by hydrothermal and hydrothermal microwave methods. Iraqi Journal of Science،Vol. 56, no. 2C, pp.1572-1587.
https://search.emarefa.net/detail/BIM-606442

Modern Language Association (MLA)

Abd al-Ghani, Ahlam Jamil& al-Ukaydi, Walid Mazlum. Preparation and characterization of yttrium oxide nanoparticles at different calcination temperatures from yttrium hydroxide prepared by hydrothermal and hydrothermal microwave methods. Iraqi Journal of Science Vol. 56, no. 2C (2015), pp.1572-1587.
https://search.emarefa.net/detail/BIM-606442

American Medical Association (AMA)

Abd al-Ghani, Ahlam Jamil& al-Ukaydi, Walid Mazlum. Preparation and characterization of yttrium oxide nanoparticles at different calcination temperatures from yttrium hydroxide prepared by hydrothermal and hydrothermal microwave methods. Iraqi Journal of Science. 2015. Vol. 56, no. 2C, pp.1572-1587.
https://search.emarefa.net/detail/BIM-606442

Data Type

Journal Articles

Language

English

Notes

Text in English ; abstracts in English and Arabic.

Record ID

BIM-606442