Preparation, identification and biological activity of a new ligand (n,n'-bis (4-Acetamidobenzalidene)‎1,3-diaminopropane)‎ with some transition metal complexes

Other Title(s)

تحضير و تشخيص و فعالية بايلوجية لليكاند جديد [N,N -بس4- أستيمدوبنزليدين)‎ 3,1-دايأمنبو برومان] و معتقداتة مع بعض العناصر الانتقالية

Joint Authors

Abd al-Rida, Maryam Ulwan
Mahdi, Haydar Abbas

Source

University of Thi-Qar Journal

Issue

Vol. 9, Issue 1 (31 Mar. 2014), pp.42-52, 11 p.

Publisher

University of Thi-Qar Research and Development Department

Publication Date

2014-03-31

Country of Publication

Iraq

No. of Pages

11

Main Subjects

Chemistry

Topics

Abstract AR

The Schiff base (N,N'-bis (4- Acetamidobenzalidene)1,3-diaminoprobane)was prepared from 4-acetaminobenzaldehyde and 1,3-diaminobrobane by refluxing the two components in methanolic solution.

The metal complexes of Fe(III),Cr(III) Co (II) and Ni (II), were prepared by mixing and refluxing ethanolic solutions of CoCl2.

6H2O,FeCl3.6H2O, CrCl3.6H2Oand NiCl2.6H2O with(N,N'-bis (4- Acetmidobenzalidene)1,3 diaminobrobane).The ligand(L)characterized by Elemental Micro Analysis (CHN) and Nuclear Magnetic Resonance Spectroscopy (1H-NMR) .The ligand(L) and it metal complexes were prepared and characterized by different techniques, such as infrared(IR) (using KBr disc to ligand and CsBr disc to complexes), Mass spectra, and (UV-vis) spectra.The complexes for ligand have shown octahedral configuration, the ligand coordinates with metal through Oxygen and Nitrogen atoms for all complexes and with ratio (1:1).

All the synthesized compounds were tested for their antibacterial activity against Escherichiacoli and Staphylococcus aureusbacteria.

American Psychological Association (APA)

Abd al-Rida, Maryam Ulwan& Mahdi, Haydar Abbas. 2014. Preparation, identification and biological activity of a new ligand (n,n'-bis (4-Acetamidobenzalidene)1,3-diaminopropane) with some transition metal complexes. University of Thi-Qar Journal،Vol. 9, no. 1, pp.42-52.
https://search.emarefa.net/detail/BIM-657575

Modern Language Association (MLA)

Abd al-Rida, Maryam Ulwan& Mahdi, Haydar Abbas. Preparation, identification and biological activity of a new ligand (n,n'-bis (4-Acetamidobenzalidene)1,3-diaminopropane) with some transition metal complexes. University of Thi-Qar Journal Vol. 9, no. 1 (Mar. 2014), pp.42-52.
https://search.emarefa.net/detail/BIM-657575

American Medical Association (AMA)

Abd al-Rida, Maryam Ulwan& Mahdi, Haydar Abbas. Preparation, identification and biological activity of a new ligand (n,n'-bis (4-Acetamidobenzalidene)1,3-diaminopropane) with some transition metal complexes. University of Thi-Qar Journal. 2014. Vol. 9, no. 1, pp.42-52.
https://search.emarefa.net/detail/BIM-657575

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references : p. 51-52

Record ID

BIM-657575