Synthesis and characterization of some mixed-ligand complexes containing Azo Dye and 1, 10-phenanthroline with CoII, ZnII, CdII and HgII Ions
Other Title(s)
تحضير و تشخيص معقدات حاوية على ليكندات مختلطة من صبغة الازو و 1,10- فينانثرولين مع أيونات الكوبلت، الكادميوم، الخارصين، الزئبق الثنائية التكافؤ
Joint Authors
Abbas, Wasan Muhammad Ulwan
Ahmad, Riyad Mahmud
Yusuf, Inam Ismail
Hasan, Hasan Ahmad
Source
Ibn al-Haitham Journal for Pure and Applied Science
Issue
Vol. 28, Issue 3 (31 Dec. 2015), pp.187-203, 17 p.
Publisher
University of Baghdad College of Education for Pure Science / Ibn al-Haitham
Publication Date
2015-12-31
Country of Publication
Iraq
No. of Pages
17
Main Subjects
Topics
Abstract EN
In this work, the ligand was obtained from the reaction of diazonium salt of naphthyl amine with 1-amino-2-naphtol-4-sulfonic acid.
The bidentate ligand type (NO) donar atoms was reacted with 1,10-phenanthroline and matel salt in a 1:1:1 mole ratio to give the complexes, using NaOH as a base.
Physical-chemical teqnichas were used to characteriz the prepared compounds FT-IR,U.V-Vis, fluorescence and 1HNMR spectroscopy, atomic absorption , chloride content along with conductivity and melting point measurements .Finally, thermal analysis was used to confirm the presence of coordination H2O molecule in the complexes structure.
According to memtioned characterization methods, the general formula proposed for CoII ZnII, CdII and HgII complexes is [M(L)(phen)(H2O)Cl].
American Psychological Association (APA)
Hasan, Hasan Ahmad& Abbas, Wasan Muhammad Ulwan& Ahmad, Riyad Mahmud& Yusuf, Inam Ismail. 2015. Synthesis and characterization of some mixed-ligand complexes containing Azo Dye and 1, 10-phenanthroline with CoII, ZnII, CdII and HgII Ions. Ibn al-Haitham Journal for Pure and Applied Science،Vol. 28, no. 3, pp.187-203.
https://search.emarefa.net/detail/BIM-679139
Modern Language Association (MLA)
Hasan, Hasan Ahmad…[et al.]. Synthesis and characterization of some mixed-ligand complexes containing Azo Dye and 1, 10-phenanthroline with CoII, ZnII, CdII and HgII Ions. Ibn al-Haitham Journal for Pure and Applied Science Vol. 28, no. 3 (2015), pp.187-203.
https://search.emarefa.net/detail/BIM-679139
American Medical Association (AMA)
Hasan, Hasan Ahmad& Abbas, Wasan Muhammad Ulwan& Ahmad, Riyad Mahmud& Yusuf, Inam Ismail. Synthesis and characterization of some mixed-ligand complexes containing Azo Dye and 1, 10-phenanthroline with CoII, ZnII, CdII and HgII Ions. Ibn al-Haitham Journal for Pure and Applied Science. 2015. Vol. 28, no. 3, pp.187-203.
https://search.emarefa.net/detail/BIM-679139
Data Type
Journal Articles
Language
English
Notes
Includes appendix : p. 194-202
Record ID
BIM-679139