Synthesis and characterization of nanocrystalline micro-mesoporous ZSM-5 MCM-41 composite zeolite

Joint Authors

Salih, Asir Abd al-Jabbar
Majid, Najwa Sabir

Source

Iraqi Journal of Chemical and Petroleum Engineering

Issue

Vol. 17, Issue 1 (31 Mar. 2016), pp.71-82, 12 p.

Publisher

University of Baghdad College of Engineering

Publication Date

2016-03-31

Country of Publication

Iraq

No. of Pages

12

Main Subjects

Chemistry

Abstract EN

Nanocrystalline micro-mesoporous ZSM/MCM-41 composite was synthesized using alkaline treatment method and two step of crystallization in poly tetraflouroethylene (PTFE) lined autoclave.

The synthesized zeolites was characterized by X-Ray diffraction (XRD), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Atomic force microscopy (AFM), Fourier transport infrared (FTIR), and N2 adsorption-desorption (BET).

It was approved that the best results for alkaline leaching can be got with 1.5M NaOH solution.

High surface (BET) area of 630 m2/g with pore volume of 0.55 cm3/g has been got.

AFM reports showed a nano-level size for average particle size of 50nm.

American Psychological Association (APA)

Majid, Najwa Sabir& Salih, Asir Abd al-Jabbar. 2016. Synthesis and characterization of nanocrystalline micro-mesoporous ZSM-5 MCM-41 composite zeolite. Iraqi Journal of Chemical and Petroleum Engineering،Vol. 17, no. 1, pp.71-82.
https://search.emarefa.net/detail/BIM-682758

Modern Language Association (MLA)

Majid, Najwa Sabir& Salih, Asir Abd al-Jabbar. Synthesis and characterization of nanocrystalline micro-mesoporous ZSM-5 MCM-41 composite zeolite. Iraqi Journal of Chemical and Petroleum Engineering Vol. 17, no. 1 (Mar. 2016), pp.71-82.
https://search.emarefa.net/detail/BIM-682758

American Medical Association (AMA)

Majid, Najwa Sabir& Salih, Asir Abd al-Jabbar. Synthesis and characterization of nanocrystalline micro-mesoporous ZSM-5 MCM-41 composite zeolite. Iraqi Journal of Chemical and Petroleum Engineering. 2016. Vol. 17, no. 1, pp.71-82.
https://search.emarefa.net/detail/BIM-682758

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references : p. 81-82

Record ID

BIM-682758