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Preperation and characterization of 1, 3-bis (methylsalicylate5-yl diazo) benzene and its complexes with some of first period transition metals
Other Title(s)
1,3-Bis (methylsalicylate5-yl diazo)benzene تحضير و تشخيص مع معقداته لبعض عناصر الدورة الانتقالية الأولى
Author
Source
Ibn al-Haitham Journal for Pure and Applied Science
Issue
Vol. 29, Issue 1 (30 Apr. 2016), pp.113-124, 12 p.
Publisher
University of Baghdad College of Education for Pure Science / Ibn al-Haitham
Publication Date
2016-04-30
Country of Publication
Iraq
No. of Pages
12
Main Subjects
Topics
Abstract EN
In this study azo dye was prepared by the reaction of m-phenylendidiazonium chloride with methyl salicylate, the resultant compound was used as a ligand for complex formation with Fe+2, Cu+2, Zn+2, Ni+2 and Co+2 ions.
The prepared ligand was characterized by H1NMR, UV-Vis., And FTIR spectroscopy, CHN analysis, in addition the complexes were characterized by TGA, UV-Vis., FTIR and conductivity methods.
The results indicate that the ligand chelated through phenoxy and carboxyl groups as a O4 quadra dentate ligand, the Co complex complet its hexagon coordination by bonding with chlorine and the complex wouid be electrolytic in opposite with rest complexes.
American Psychological Association (APA)
Sultan, Khawlah Muhammad. 2016. Preperation and characterization of 1, 3-bis (methylsalicylate5-yl diazo) benzene and its complexes with some of first period transition metals. Ibn al-Haitham Journal for Pure and Applied Science،Vol. 29, no. 1, pp.113-124.
https://search.emarefa.net/detail/BIM-692470
Modern Language Association (MLA)
Sultan, Khawlah Muhammad. Preperation and characterization of 1, 3-bis (methylsalicylate5-yl diazo) benzene and its complexes with some of first period transition metals. Ibn al-Haitham Journal for Pure and Applied Science Vol. 29, no. 1 (2016), pp.113-124.
https://search.emarefa.net/detail/BIM-692470
American Medical Association (AMA)
Sultan, Khawlah Muhammad. Preperation and characterization of 1, 3-bis (methylsalicylate5-yl diazo) benzene and its complexes with some of first period transition metals. Ibn al-Haitham Journal for Pure and Applied Science. 2016. Vol. 29, no. 1, pp.113-124.
https://search.emarefa.net/detail/BIM-692470
Data Type
Journal Articles
Language
English
Notes
Includes appendices : p. 119-123
Record ID
BIM-692470