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Preparation and characterization of new mixed ligand complexes of (p-methyl anilino)-p-chloro phenyl acetonitrile and ethylene diamine
Other Title(s)
تحضير و تشخيص معقدات فلزية جديدة لخليط الليكاندين (بارامثيل انيلينو)-باراكلوروفنيل اسيتونتريل و اثيلين ثنائي أمين
Author
Source
Issue
Vol. 57, Issue 4B (31 Dec. 2016), pp.2592-2603, 12 p.
Publisher
University of Baghdad College of Science
Publication Date
2016-12-31
Country of Publication
Iraq
No. of Pages
12
Main Subjects
Topics
Abstract EN
New mixed ligand complexes of some metal ions Zn(II), Cd(II) and Hg(II) were prepared by reacting with mixture of two bidentate ligands [ HL = (P-methyl anilino) –P– chloro phenyl acetonitrile and en = ethylene diamine] in a molar ratio of 1:1:1[ M : HL : en] in ethanol .
The ligand HL was previously prepared by Strecker’s procedure which includes the reaction of p- toluidine with P- chlorobenzaldehyde in the presence of KCN in acidic medium.
The structures of new compounds were identified by elemental analyses, atomic absorption and thermal analyses TG/DTG in addition to FTIR and U.V-VIS.
Spectra.
The electrical conductivity measurements of metal complexes were also determined.
From the obtained data the octahedral structure was suggested for all prepared complexes
American Psychological Association (APA)
Majid, Rawa Abbas. 2016. Preparation and characterization of new mixed ligand complexes of (p-methyl anilino)-p-chloro phenyl acetonitrile and ethylene diamine. Iraqi Journal of Science،Vol. 57, no. 4B, pp.2592-2603.
https://search.emarefa.net/detail/BIM-728819
Modern Language Association (MLA)
Majid, Rawa Abbas. Preparation and characterization of new mixed ligand complexes of (p-methyl anilino)-p-chloro phenyl acetonitrile and ethylene diamine. Iraqi Journal of Science Vol. 57, no. 4B (2016), pp.2592-2603.
https://search.emarefa.net/detail/BIM-728819
American Medical Association (AMA)
Majid, Rawa Abbas. Preparation and characterization of new mixed ligand complexes of (p-methyl anilino)-p-chloro phenyl acetonitrile and ethylene diamine. Iraqi Journal of Science. 2016. Vol. 57, no. 4B, pp.2592-2603.
https://search.emarefa.net/detail/BIM-728819
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 2602-2603
Record ID
BIM-728819