Synthesis, structural and spectroscopic study of complexes of tetradentate schiff base derived from malonyl dihydrazide with Cr (III), Mn (II), Co (II), Cu (II) and Zn (II) ions
Author
al-Bayati, Sinan Midhat Muhammad
Source
Engineering and Technology Journal
Issue
Vol. 35, Issue 1B (31 Jan. 2017), pp.50-56, 7 p.
Publisher
Publication Date
2017-01-31
Country of Publication
Iraq
No. of Pages
7
Main Subjects
Engineering & Technology Sciences (Multidisciplinary)
Abstract EN
This paper describes the synthesis of a new derivative dihydro-3H-indol-3-ylidene propane dihydrazide [L], which have been obtained from the reaction between malonyl di-hydrazide and an ethanollic solution of isatin.
Tetradentatemacrocyclic ligand [L] was characterized by (C.H.N), (FT-IR), (UV-Vis), and 1H.NMR.A series of the used metal complexes have been synthesized by the prepared ligand [L] reaction with some transition metal ions.
The isolated complexes were Cr(III), Mn(II), Co(II), Ni(II), Cu(II) and Zn(II) also characterized using different techniques such as (FT-IR), and (UV-Vis) spectroscopies, (C.H.N), flam atomic absorption in addition to the magnetic susceptibility and molar conductivity measurement.
Al complexes were octahedral in geometry except for Zn (II) complex, which was tetrahedral.
American Psychological Association (APA)
al-Bayati, Sinan Midhat Muhammad. 2017. Synthesis, structural and spectroscopic study of complexes of tetradentate schiff base derived from malonyl dihydrazide with Cr (III), Mn (II), Co (II), Cu (II) and Zn (II) ions. Engineering and Technology Journal،Vol. 35, no. 1B, pp.50-56.
https://search.emarefa.net/detail/BIM-770020
Modern Language Association (MLA)
al-Bayati, Sinan Midhat Muhammad. Synthesis, structural and spectroscopic study of complexes of tetradentate schiff base derived from malonyl dihydrazide with Cr (III), Mn (II), Co (II), Cu (II) and Zn (II) ions. Engineering and Technology Journal Vol. 35, no. 1B (2017), pp.50-56.
https://search.emarefa.net/detail/BIM-770020
American Medical Association (AMA)
al-Bayati, Sinan Midhat Muhammad. Synthesis, structural and spectroscopic study of complexes of tetradentate schiff base derived from malonyl dihydrazide with Cr (III), Mn (II), Co (II), Cu (II) and Zn (II) ions. Engineering and Technology Journal. 2017. Vol. 35, no. 1B, pp.50-56.
https://search.emarefa.net/detail/BIM-770020
Data Type
Journal Articles
Language
English
Notes
Includes appendix : p. 56
Record ID
BIM-770020