Synthesis of some new 2-thioxoimidazolidin-4-one derivatives : (part I)
Other Title(s)
تحضير بعض المشتقات الجديدة من 2-ثايوكسواميدازولدين-4-اون
Author
Source
Ibn al-Haitham Journal for Pure and Applied Science
Issue
Vol. 29, Issue 3 (31 Dec. 2016), pp.88-102, 15 p.
Publisher
University of Baghdad College of Education for Pure Science / Ibn al-Haitham
Publication Date
2016-12-31
Country of Publication
Iraq
No. of Pages
15
Main Subjects
Topics
Abstract EN
This research includes the synthesis of new series of heterocyclic compounds.
Reaction of 2-nitro benzylidene thiosemicarbazide(1) with ethyl chloro acetate gave (2-nitro benzylidene amino)-2-thioxomidazolidine-4-one(2) ,treatment(2) with methyl iodide to give(3)which was reacted with hydrazine to give 2-hydrazinyl-1-[(2-nitrobenzylidene)amino]- 1H-imidazol-5(4H)-one, andreation of compound(2) with aromatic aldehydes to give 5-arylidene -3-({2-nitro benzylidene}amino)2-thioxo-3,5-dihydro-4H-imidazole-4-one(5a,5b), which was reacted with ethyl aceto acetate to give 4-aryl-1-[2-nitrobenzylidene, amino -6-oxo-2-thioxo octa hydro-1H-benzo[d]imidazole-5-carboxylate and followed synthesis of β-lactamederivtives(9a,9b) by treatment derivatives(8a,8b)schiff bases with chloro acetyl chloride .some new compounds were characterized by of some protone NMR of them and IR spectroscopy.
American Psychological Association (APA)
Ulaywi, Amjad Ghali. 2016. Synthesis of some new 2-thioxoimidazolidin-4-one derivatives : (part I). Ibn al-Haitham Journal for Pure and Applied Science،Vol. 29, no. 3, pp.88-102.
https://search.emarefa.net/detail/BIM-774802
Modern Language Association (MLA)
Ulaywi, Amjad Ghali. Synthesis of some new 2-thioxoimidazolidin-4-one derivatives : (part I). Ibn al-Haitham Journal for Pure and Applied Science Vol. 29, no. 3 (2016), pp.88-102.
https://search.emarefa.net/detail/BIM-774802
American Medical Association (AMA)
Ulaywi, Amjad Ghali. Synthesis of some new 2-thioxoimidazolidin-4-one derivatives : (part I). Ibn al-Haitham Journal for Pure and Applied Science. 2016. Vol. 29, no. 3, pp.88-102.
https://search.emarefa.net/detail/BIM-774802
Data Type
Journal Articles
Language
English
Notes
Includes appendices : p. 99-101
Record ID
BIM-774802