Preparation, identification and biological activity of a new ligand (N, N'-bis (4-Acetamidobenzalidene)1,3-diaminopropane) with some transition metal complexes
Other Title(s)
بس 4-استميدو بنزليدين) 1,3-داي-N, N) تحضير و تشخيص و فعالية بايلوجية لليكاند جديد امنيو بروبان و معقداته مع بعض العناصر الانتقالية
Joint Authors
Abd al-Rida, Maryam Ulwan
Mahdi, Haydar Abbas
Source
Issue
Vol. 11, Issue 1 (31 Mar. 2016), pp.42-52, 11 p.
Publisher
University of Thi-Qar Research and Development Department
Publication Date
2016-03-31
Country of Publication
Iraq
No. of Pages
11
Main Subjects
Topics
Abstract EN
-The Schiff base (N,N'-bis (4- Acetamidobenzalidene)1,3-diaminoprobane)was prepared from 4-acetaminobenzaldehyde and 1,3-diaminobrobane by refluxing the two components in methanolic solution.
The metal complexes of Fe(III),Cr(III) Co (II) and Ni (II), were prepared by mixing and refluxing ethanolic solutions of CoCl2. 6H2O,FeCl3.6H2O, CrCl3.6H2Oand NiCl2.6H2O with(N,N'-bis (4- Acetmidobenzalidene)1,3 diaminobrobane).The ligand(L)characterized by Elemental Micro Analysis (CHN) and Nuclear Magnetic Resonance Spectroscopy (1H-NMR) .The ligand(L) and it metal complexes were prepared and characterized by different techniques, such as infrared(IR) (using KBr disc to ligand and CsBr disc to complexes), Mass spectra, and (UV-vis) spectra.The complexes for ligand have shown octahedral configuration, the ligand coordinates with metal through Oxygen and Nitrogen atoms for all complexes and with ratio (1:1).
All the synthesized compounds were tested for their antibacterial activity against Escherichiacoli and Staphylococcus aureusbacteria
American Psychological Association (APA)
Abd al-Rida, Maryam Ulwan& Mahdi, Haydar Abbas. 2016. Preparation, identification and biological activity of a new ligand (N, N'-bis (4-Acetamidobenzalidene)1,3-diaminopropane) with some transition metal complexes. University of Thi-Qar Journal،Vol. 11, no. 1, pp.42-52.
https://search.emarefa.net/detail/BIM-786294
Modern Language Association (MLA)
Abd al-Rida, Maryam Ulwan& Mahdi, Haydar Abbas. Preparation, identification and biological activity of a new ligand (N, N'-bis (4-Acetamidobenzalidene)1,3-diaminopropane) with some transition metal complexes. University of Thi-Qar Journal Vol. 11, no. 1 (Mar. 2016), pp.42-52.
https://search.emarefa.net/detail/BIM-786294
American Medical Association (AMA)
Abd al-Rida, Maryam Ulwan& Mahdi, Haydar Abbas. Preparation, identification and biological activity of a new ligand (N, N'-bis (4-Acetamidobenzalidene)1,3-diaminopropane) with some transition metal complexes. University of Thi-Qar Journal. 2016. Vol. 11, no. 1, pp.42-52.
https://search.emarefa.net/detail/BIM-786294
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 51-52
Record ID
BIM-786294