Synthesis and characterization of Schiff base ((2S)‎-3-phenyl-2-((E)‎-((1S)‎-1, 7, 7-trimethylbicyclo [2. 2. 1] heptan-2-ylidene)‎ amino)‎ propanoic acid)‎ and their metal complexes

Other Title(s)

)‎(2S)‎-3-phenyl-2-((E)‎-((1S)‎-تحضير و تشخيص قاعدة شيف- 1,7,7 trimethylbicyclo (2.2.1)‎ heptan-2-ylidene)‎amino)‎ propanoic و معقداتها الفلزية acid)‎

Author

al-Sadawi, Nuha Husayn

Source

University of Thi-Qar Journal

Issue

Vol. 12, Issue 1 (31 Mar. 2017), pp.111-129, 19 p.

Publisher

University of Thi-Qar Research and Development Department

Publication Date

2017-03-31

Country of Publication

Iraq

No. of Pages

19

Main Subjects

Chemistry

Topics

Abstract EN

The reaction of camphor with phenylalanine under showed conditions yielded Schiff base as a ligand.

The structures of Cu(II), Ni(II), Co(II) and Fe(II) with schiff base compound have been joined by the reacting between copper bromide, hexahydrate nickel chloride, hexahydrate cobalt chloride and iron bromide and ligand in 1:2 mole ratio.

The free ligand and their metal structures have been in the solid state.

The spectroscopic data of the structures suggest their 1:2 buildings structures which are inspected by elemental analysis (CHN), FT-IR, 1H NMR spectroscopy.

The spectroscopic studies proposed the octahedral structure for the all structures and the results are represented and analyzed underneath.

American Psychological Association (APA)

al-Sadawi, Nuha Husayn. 2017. Synthesis and characterization of Schiff base ((2S)-3-phenyl-2-((E)-((1S)-1, 7, 7-trimethylbicyclo [2. 2. 1] heptan-2-ylidene) amino) propanoic acid) and their metal complexes. University of Thi-Qar Journal،Vol. 12, no. 1, pp.111-129.
https://search.emarefa.net/detail/BIM-787792

Modern Language Association (MLA)

al-Sadawi, Nuha Husayn. Synthesis and characterization of Schiff base ((2S)-3-phenyl-2-((E)-((1S)-1, 7, 7-trimethylbicyclo [2. 2. 1] heptan-2-ylidene) amino) propanoic acid) and their metal complexes. University of Thi-Qar Journal Vol. 12, no. 1 (Mar. 2017), pp.111-129.
https://search.emarefa.net/detail/BIM-787792

American Medical Association (AMA)

al-Sadawi, Nuha Husayn. Synthesis and characterization of Schiff base ((2S)-3-phenyl-2-((E)-((1S)-1, 7, 7-trimethylbicyclo [2. 2. 1] heptan-2-ylidene) amino) propanoic acid) and their metal complexes. University of Thi-Qar Journal. 2017. Vol. 12, no. 1, pp.111-129.
https://search.emarefa.net/detail/BIM-787792

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references : p. 126-128

Record ID

BIM-787792