Synthesis and identification of new oxazepine derivatives bearing azo group in their structures
Other Title(s)
تحضير وتشخيص مشتقات جديدة للأوكسازيبين تحتوي على مجموعة الأزو في تركيبها
Joint Authors
Sallal, Zaynab Amir
Ghanim, Hasan Thamir
Source
Issue
Vol. 59, Issue 1A (31 Mar. 2018), pp.1-8, 8 p.
Publisher
University of Baghdad College of Science
Publication Date
2018-03-31
Country of Publication
Iraq
No. of Pages
8
Main Subjects
Topics
Abstract EN
In this contribution new oxazepine compounds containing azo group were preppared.
In the firststep,4-(dimethylamino)-3-((4-methoxy phenyl) diazenyl) benzaldehyde [Z] was synthesised by using 4-methoxyaniline.
The second step was the condensation reaction between aldehyde group of the azo compound [Z] and different primary aromatic amines [4-hydroxyaniline, 4-chloroaniline and 4-amino-N-(pyrimidin-2-yl) benzenesulfonamide] to yield new azo Schiff bases compounds [A1-A3] respectively.
In the final step, oxazepine compounds [B1-B3] and [B4-B6] were prepared from reaction imines compounds [A1-A3] with maleic anhydride and phathalic anhydride in dry benzene respectively.
All these derivatives were characterized by melting points and FTIR spectroscopy, some of them were characterized by 1H-NMR spectroscopy.
American Psychological Association (APA)
Sallal, Zaynab Amir& Ghanim, Hasan Thamir. 2018. Synthesis and identification of new oxazepine derivatives bearing azo group in their structures. Iraqi Journal of Science،Vol. 59, no. 1A, pp.1-8.
https://search.emarefa.net/detail/BIM-831268
Modern Language Association (MLA)
Sallal, Zaynab Amir& Ghanim, Hasan Thamir. Synthesis and identification of new oxazepine derivatives bearing azo group in their structures. Iraqi Journal of Science Vol. 59, no. 1A (2018), pp.1-8.
https://search.emarefa.net/detail/BIM-831268
American Medical Association (AMA)
Sallal, Zaynab Amir& Ghanim, Hasan Thamir. Synthesis and identification of new oxazepine derivatives bearing azo group in their structures. Iraqi Journal of Science. 2018. Vol. 59, no. 1A, pp.1-8.
https://search.emarefa.net/detail/BIM-831268
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 8
Record ID
BIM-831268