Synthesis of new bis-1,3,4-thiadiazoles substituted from benzidine containing oxazepine or benzoxazepine moieties
Joint Authors
al-Ramahi, Faiz Abd al-Husayn
Ismail, Qasim Mahdi
Source
Journal of Kufa for Chemical Science
Issue
Vol. 2, Issue 3 (31 Dec. 2017), pp.43-55, 13 p.
Publisher
University of Kufa Faculty of Education for Women Department of Chemistry
Publication Date
2017-12-31
Country of Publication
Iraq
No. of Pages
13
Main Subjects
Topics
Abstract EN
Benzidine was converted to the corresponding bis-diazonium salt which was introduced in coupling reaction with alkaline solution of 2-hydroxybenzaldehyde as coupling reagent to give bis-azo derivative (1) containing two aldehyde groups.
The resulting bis-aldehyde (1) was then introduced in condensation reaction with 2-amino-5- mercapto-1,3,4-thiadiazole to produce the bis-imine (2).Then compound (2) was reacted with maleic anhydride and phthalic anhydride to give (3a and 3b) respectively .All compounds were spectral identification by FTIR and 1HNMR.
American Psychological Association (APA)
al-Ramahi, Faiz Abd al-Husayn& Ismail, Qasim Mahdi. 2017. Synthesis of new bis-1,3,4-thiadiazoles substituted from benzidine containing oxazepine or benzoxazepine moieties. Journal of Kufa for Chemical Science،Vol. 2, no. 3, pp.43-55.
https://search.emarefa.net/detail/BIM-903473
Modern Language Association (MLA)
al-Ramahi, Faiz Abd al-Husayn& Ismail, Qasim Mahdi. Synthesis of new bis-1,3,4-thiadiazoles substituted from benzidine containing oxazepine or benzoxazepine moieties. Journal of Kufa for Chemical Science Vol. 2, no. 3 (Dec. 2017), pp.43-55.
https://search.emarefa.net/detail/BIM-903473
American Medical Association (AMA)
al-Ramahi, Faiz Abd al-Husayn& Ismail, Qasim Mahdi. Synthesis of new bis-1,3,4-thiadiazoles substituted from benzidine containing oxazepine or benzoxazepine moieties. Journal of Kufa for Chemical Science. 2017. Vol. 2, no. 3, pp.43-55.
https://search.emarefa.net/detail/BIM-903473
Data Type
Journal Articles
Language
English
Notes
Includes appendices : p. 51-55
Record ID
BIM-903473