Spectrophotometric ANN atomic absorption determination cefixime by cloud point extraction in pure form
Other Title(s)
التقدير الطيفي و الامتصاص الذري للسفكسيم بواسطة الاستخلاص بنقطة الغيمة في المادة النقية
Joint Authors
Zahir, Sadiyah Ahmad
Muhamma, Nur Jamal
Source
The Iraqi Journal of Agricultural Science
Issue
Vol. 50, Issue 5 (31 Oct. 2019), pp.1390-1404, 15 p.
Publisher
University of Baghdad College of Agriculture
Publication Date
2019-10-31
Country of Publication
Iraq
No. of Pages
15
Main Subjects
Topics
Abstract EN
A simple, rapid, accurate, sensitive and ecofriendly method has been developed for the quantitative determination of Cefixime (CFX) in pure form and pharmaceutical preparations by using a combination of cloud point extraction with UV-Visible absorption spectrophotometric method.
Analytical applications of complexation with metal ions by reacting Cefixime (CFX) with Iron (III) to form chelate complexes under limited experimental conditions.
The method based to dissolved CFX in 0.1 M NaOH, 10% (v/v) Triton X-114 and mixed with (1000 μg mL-1 ) Iron (III).
The formation of CFX- Fe (III) complex was formatted at pH 11 and wavelength at 439 nm.
The complex of CFX- Fe (III) obey Beer’s Law in the range 10-160μg/ml.
LOD and LOQ values for the complex were 1.5865 μg/ml and 5.2887 μg/ml respectively.
Method was validated and successfully applied to drug formulations like syrup infusion The results of analysis have been validated statistically and by recovery studies and were found satisfactory.
American Psychological Association (APA)
Zahir, Sadiyah Ahmad& Muhamma, Nur Jamal. 2019. Spectrophotometric ANN atomic absorption determination cefixime by cloud point extraction in pure form. The Iraqi Journal of Agricultural Science،Vol. 50, no. 5, pp.1390-1404.
https://search.emarefa.net/detail/BIM-909960
Modern Language Association (MLA)
Zahir, Sadiyah Ahmad& Muhamma, Nur Jamal. Spectrophotometric ANN atomic absorption determination cefixime by cloud point extraction in pure form. The Iraqi Journal of Agricultural Science Vol. 50, no. 5 (2019), pp.1390-1404.
https://search.emarefa.net/detail/BIM-909960
American Medical Association (AMA)
Zahir, Sadiyah Ahmad& Muhamma, Nur Jamal. Spectrophotometric ANN atomic absorption determination cefixime by cloud point extraction in pure form. The Iraqi Journal of Agricultural Science. 2019. Vol. 50, no. 5, pp.1390-1404.
https://search.emarefa.net/detail/BIM-909960
Data Type
Journal Articles
Language
English
Notes
Text in English ; abstracts in English and Arabic.
Record ID
BIM-909960