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Synthesis and characterization of Pd (II) And Pt (II) complexes with Bis [Hg (2-Apt)] compound
Other Title(s)
تحضير وتشخيص معقدات ( Pt (II), Pd (II مع مركب ثنائي [(Hg (2-apt]
Joint Authors
Amin, Beriwan Muhammad Hamad
Muhammad, Hikmat Ali
Source
Kirkuk University Journal-Scientific Studies
Issue
Vol. 13, Issue 3 (30 Sep. 2018), pp.12-22, 11 p.
Publisher
Kirkuk University College of Science
Publication Date
2018-09-30
Country of Publication
Iraq
No. of Pages
11
Main Subjects
Topics
Abstract AR
تفاعل مول واحد من خلات Hg (II) مع مولين من 2-امينوثايوفينول أعطت مول واحد من مركبا Hg (2- apt) بينما تفاعل مول واحد من [ Hg (2-apt)] مع مولين من ملح [MCl2] أنتجت معقدات جديدة ذوات الصيغة [M2 {Hg (2-apt) cl4 حيث M= Pd (II), Pt (II) ] تم تشخيص جميع المعقدات باستخدام 13C-NMR FT-IR, 1H-NMR وقياسات تحليل الدقيق للعناصر (CHNS) والمولارية.
وقد أظهرت النتائج بأن الفلز يتناسق مع الليكاند من خلال S, N مكونا شكل المربع المستوي.
Abstract EN
The reaction of one mole of Hg (II) acetate with two mole of 2-amino thiophenol gave one mole of [Hg(2-apt)] compound.
While the reaction of one mole of [Hg (2-apt)] with two moles of MCL2 salt.
Produced new complexes in general formula [M2{Hg(2-apt) Cl4] where M=Pt (II) or Pd (II).
All the prepared complexes were identified using FT-IR, 1H-NMR,13CNMR,elemental analyses (CHNS) and molar conductivity.
The results exhibited that metal bounded to the ligand via S and N in square planer geometries.
American Psychological Association (APA)
Amin, Beriwan Muhammad Hamad& Muhammad, Hikmat Ali. 2018. Synthesis and characterization of Pd (II) And Pt (II) complexes with Bis [Hg (2-Apt)] compound. Kirkuk University Journal-Scientific Studies،Vol. 13, no. 3, pp.12-22.
https://search.emarefa.net/detail/BIM-946115
Modern Language Association (MLA)
Amin, Beriwan Muhammad Hamad& Muhammad, Hikmat Ali. Synthesis and characterization of Pd (II) And Pt (II) complexes with Bis [Hg (2-Apt)] compound. Kirkuk University Journal-Scientific Studies Vol. 13, no. 3 (Sep. 2018), pp.12-22.
https://search.emarefa.net/detail/BIM-946115
American Medical Association (AMA)
Amin, Beriwan Muhammad Hamad& Muhammad, Hikmat Ali. Synthesis and characterization of Pd (II) And Pt (II) complexes with Bis [Hg (2-Apt)] compound. Kirkuk University Journal-Scientific Studies. 2018. Vol. 13, no. 3, pp.12-22.
https://search.emarefa.net/detail/BIM-946115
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 20-22
Record ID
BIM-946115