Synthesis, spectral studies and antimicrobial evaluation of 6,6--(1,2-benzenediazo) bis (3-amino benzoic acid) complexes with some metal ions
Other Title(s)
تحضير، دراسة طيفية وتقييم الفعالية البايولوجية لمعقدات -1،2 )-6،6بنزين آزو( ثنائي ( -3امينو حامض البنزويك) مع بعض الأيونات الفلزية
Joint Authors
al-Hutaymi, Zafir Tamuin ujayl
Muhammad, Sahad Shakir
Abd al-Amir, Nibras
Jarad, Amir Jabbar
Source
Journal of al-Qadisiyah for Pure Science
Issue
Vol. 20, Issue 1 (31 Mar. 2015), pp.148-159, 12 p.
Publisher
al-Qadisiyah University College of Science
Publication Date
2015-03-31
Country of Publication
Iraq
No. of Pages
12
Main Subjects
Abstract EN
The Ligand 6,6--(1,2-benzenediazo) bis (3-aminobenzoicacid) derived from o-phenylenediamine and 3-aminobenzoicacid was synthesized.
The prepared ligand was identified by Microelemental Analysis, 1HNMR, FT-IR and UV-Vis spectroscopic techniques.
Treatment of the ligand with the following metal ions (CoII, NiII, CuII and ZnII ) in aqueous ethanol with a 1:1 M:L ratio and at optimum pH.
Characterization of these compounds has been done on the basis of elemental analysis, electronic data, FT-IR and UV-Vis, as well as magnetic susceptibility and conductivity measurements.
The nature of the complexes formed were studied following the mole ratio and continuous variation methods, Beer's law obeyed over a concentration range (1×10-4 - 3×10-4 M).
High molar absorbtivity of the complex solutions were observed.
On the basis of physicochemical data tetrahedral geometries were assigned for the complexes.
The ligand and metal complexes were screened for their antimicrobial activity.
American Psychological Association (APA)
Jarad, Amir Jabbar& Abd al-Amir, Nibras& Muhammad, Sahad Shakir& al-Hutaymi, Zafir Tamuin ujayl. 2015. Synthesis, spectral studies and antimicrobial evaluation of 6,6--(1,2-benzenediazo) bis (3-amino benzoic acid) complexes with some metal ions. Journal of al-Qadisiyah for Pure Science،Vol. 20, no. 1, pp.148-159.
https://search.emarefa.net/detail/BIM-949393
Modern Language Association (MLA)
Jarad, Amir Jabbar…[et al.]. Synthesis, spectral studies and antimicrobial evaluation of 6,6--(1,2-benzenediazo) bis (3-amino benzoic acid) complexes with some metal ions. Journal of al-Qadisiyah for Pure Science Vol. 20, no. 1 (2015), pp.148-159.
https://search.emarefa.net/detail/BIM-949393
American Medical Association (AMA)
Jarad, Amir Jabbar& Abd al-Amir, Nibras& Muhammad, Sahad Shakir& al-Hutaymi, Zafir Tamuin ujayl. Synthesis, spectral studies and antimicrobial evaluation of 6,6--(1,2-benzenediazo) bis (3-amino benzoic acid) complexes with some metal ions. Journal of al-Qadisiyah for Pure Science. 2015. Vol. 20, no. 1, pp.148-159.
https://search.emarefa.net/detail/BIM-949393
Data Type
Journal Articles
Language
English
Notes
Record ID
BIM-949393