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A Confirmatory Method Based on HPLC-MSMS for the Detection and Quantification of Residue of Tetracyclines in Nonmedicated Feed
المؤلفون المشاركون
Cepeda, Alberto
Gavilán, Rosa E.
Nebot, Carolina
Veiga-Gómez, Maria
Roca-Saavedra, Paula
Vazquez Belda, Beatriz
Franco, Carlos M.
المصدر
Journal of Analytical Methods in Chemistry
العدد
المجلد 2016، العدد 2016 (31 ديسمبر/كانون الأول 2016)، ص ص. 1-8، 8ص.
الناشر
Hindawi Publishing Corporation
تاريخ النشر
2016-08-09
دولة النشر
مصر
عدد الصفحات
8
التخصصات الرئيسية
الملخص EN
The Commission Regulation 574/2011/EC set up maximum levels of coccidiostats and histomonostats in nonmedicated feed as a consequence of carry-over during manufacturing.
Carry-over takes place from medicated to nonmedicated feed during feed production.
Similar contamination could also occur for other pharmaceuticals such as tetracyclines, a group of antibiotics commonly employed in food production animal.
The objective of this work is to present a simple and fast method for the simultaneous detection of four tetracyclines (chlortetracycline, doxycycline, oxytetracycline, and tetracycline) in nontarget feed at a μg/kg level.
Validation of the method was performed according to the guideline included in the Commission Decision 2002/657/EC for official method.
The validated method was successfully applied to 50 feed samples collected from different milk farms and 25 samples obtained from feed manufacturers.
While oxytetracycline was the tetracycline most frequently detected, chlortetracycline was the analyte measured at the highest concentration 15.14 mg/Kg.
From 75 nonmedicated feed analysed 15% resulted to be positive for the presence of one tetracycline.
نمط استشهاد جمعية علماء النفس الأمريكية (APA)
Gavilán, Rosa E.& Nebot, Carolina& Veiga-Gómez, Maria& Roca-Saavedra, Paula& Vazquez Belda, Beatriz& Franco, Carlos M.…[et al.]. 2016. A Confirmatory Method Based on HPLC-MSMS for the Detection and Quantification of Residue of Tetracyclines in Nonmedicated Feed. Journal of Analytical Methods in Chemistry،Vol. 2016, no. 2016, pp.1-8.
https://search.emarefa.net/detail/BIM-1107258
نمط استشهاد الجمعية الأمريكية للغات الحديثة (MLA)
Gavilán, Rosa E.…[et al.]. A Confirmatory Method Based on HPLC-MSMS for the Detection and Quantification of Residue of Tetracyclines in Nonmedicated Feed. Journal of Analytical Methods in Chemistry No. 2016 (2016), pp.1-8.
https://search.emarefa.net/detail/BIM-1107258
نمط استشهاد الجمعية الطبية الأمريكية (AMA)
Gavilán, Rosa E.& Nebot, Carolina& Veiga-Gómez, Maria& Roca-Saavedra, Paula& Vazquez Belda, Beatriz& Franco, Carlos M.…[et al.]. A Confirmatory Method Based on HPLC-MSMS for the Detection and Quantification of Residue of Tetracyclines in Nonmedicated Feed. Journal of Analytical Methods in Chemistry. 2016. Vol. 2016, no. 2016, pp.1-8.
https://search.emarefa.net/detail/BIM-1107258
نوع البيانات
مقالات
لغة النص
الإنجليزية
الملاحظات
Includes bibliographical references
رقم السجل
BIM-1107258
قاعدة معامل التأثير والاستشهادات المرجعية العربي "ارسيف Arcif"
أضخم قاعدة بيانات عربية للاستشهادات المرجعية للمجلات العلمية المحكمة الصادرة في العالم العربي
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