Synthesis of MIL-100(Fe)‎ at Low Temperature and Atmospheric Pressure

المؤلفون المشاركون

Shi, Jing
Zhang, Fumin
Zhong, Yijun
Liu, Huanhuan
Fu, Yanghe
Hei, Shengtao
Zhu, Weidong

المصدر

Journal of Chemistry

العدد

المجلد 2013، العدد 2013 (31 ديسمبر/كانون الأول 2013)، ص ص. 1-4، 4ص.

الناشر

Hindawi Publishing Corporation

تاريخ النشر

2013-10-03

دولة النشر

مصر

عدد الصفحات

4

التخصصات الرئيسية

الكيمياء

الملخص EN

MIL-100(Fe), a mesoporous metal-organic framework (MOF), has a large BET specific surface area and pore volume with the presence of a significant amount of accessible Lewis acid metal sites upon dehydration.

The structural characteristics of MIL-100(Fe) make it a good candidate for potential applications in gas storage, separation, and heterogeneous catalysis.

Mainly, this MOF is obtained by the hydrothermal synthesis in a Teflon-lined autoclave at high temperature (>150°C) under static conditions.

However, this method has several disadvantages such as high temperature, high (autogenous) pressure, long time, and comparable low MOF yield.

Therefore, development of a facile method for synthesis of MIL-100(Fe) is vitally important for fundamental understanding and practical application.

Herein, MIL-100(Fe) is synthesized by a facile low-temperature (<100°C) synthesis route at atmospheric pressure by reaction of metallic iron and trimesic acid in water.

Due to our synthesis is conducted with agitation, higher MOF yield (>90%) still could be achieved, suggesting that this simple and energy saving method has the potential to be used practically.

نمط استشهاد جمعية علماء النفس الأمريكية (APA)

Shi, Jing& Hei, Shengtao& Liu, Huanhuan& Fu, Yanghe& Zhang, Fumin& Zhong, Yijun…[et al.]. 2013. Synthesis of MIL-100(Fe) at Low Temperature and Atmospheric Pressure. Journal of Chemistry،Vol. 2013, no. 2013, pp.1-4.
https://search.emarefa.net/detail/BIM-498519

نمط استشهاد الجمعية الأمريكية للغات الحديثة (MLA)

Shi, Jing…[et al.]. Synthesis of MIL-100(Fe) at Low Temperature and Atmospheric Pressure. Journal of Chemistry No. 2013 (2013), pp.1-4.
https://search.emarefa.net/detail/BIM-498519

نمط استشهاد الجمعية الطبية الأمريكية (AMA)

Shi, Jing& Hei, Shengtao& Liu, Huanhuan& Fu, Yanghe& Zhang, Fumin& Zhong, Yijun…[et al.]. Synthesis of MIL-100(Fe) at Low Temperature and Atmospheric Pressure. Journal of Chemistry. 2013. Vol. 2013, no. 2013, pp.1-4.
https://search.emarefa.net/detail/BIM-498519

نوع البيانات

مقالات

لغة النص

الإنجليزية

الملاحظات

Includes bibliographical references

رقم السجل

BIM-498519