Design and synthesis of two triazoninecarbaldehyde derivatives using several chemical tools
المؤلفون المشاركون
Figueroa Valverde, Lauro
Dıaz Cedillo, Francisco, Francisco
Garcıa Cervera, Elodia
Pool Gomez, Eduardo
Rosas Nexticapa, Marcela
Lopez Ramos, Marıa
Vera Escobedo, Maria Isabel
المصدر
Journal of Saudi Chemical Society
العدد
المجلد 22، العدد 2 (28 فبراير/شباط 2018)، ص ص. 183-197، 15ص.
الناشر
تاريخ النشر
2018-02-28
دولة النشر
السعودية
عدد الصفحات
15
التخصصات الرئيسية
الملخص EN
Several triazonine-carbaldehyde derivatives have been prepared using different protocols ; however, some require special reagents and conditions.
The aim of study involved the synthesis of two triazonine-carbaldehyde derivative using testosterone or OTBS-testosterone as chemical tool.
Triazonine-carbaldehyde derivatives were prepared by a series of reactions that involve the following : (1) synthesis of two nitrobenzamide derivatives by reaction of testosterone or OTBS-testosterone with p-nitrobenzoyl azide using Copper(II) as catalyst ; (2) reaction of the nitrobenzamides with ethylenediamine to form two triazonine derivatives using boric acid as catalyst; (3) preparation of hexynyl-triazonine derivatives by the reaction of two triazonines 6-chlorohex-1-yne in basic medium ; (4) reaction of hexynyl-triazonine derivatives with benzaldehyde to form two triazoninol analogs ; (5) preparation of triazoninynal derivatives through oxidation of triazoninol analogs with dimethyl sulfoxide ; and (6) synthesis of triazonine-carbaldehyde derivatives by the reaction of triazoninynal derivatives with hexyne-1 using Copper(II) as catalyst.
The chemical structure of compounds was determined by spectroscopic and spectrometric methods.
In conclusion, in this work were prepared two triazoninone derivatives using several hemical techniques, which are simple procedures and easy to handle.
نمط استشهاد جمعية علماء النفس الأمريكية (APA)
Figueroa Valverde, Lauro& Dıaz Cedillo, Francisco, Francisco& Garcıa Cervera, Elodia& Pool Gomez, Eduardo& Rosas Nexticapa, Marcela& Lopez Ramos, Marıa…[et al.]. 2018. Design and synthesis of two triazoninecarbaldehyde derivatives using several chemical tools. Journal of Saudi Chemical Society،Vol. 22, no. 2, pp.183-197.
https://search.emarefa.net/detail/BIM-782277
نمط استشهاد الجمعية الأمريكية للغات الحديثة (MLA)
Figueroa Valverde, Lauro…[et al.]. Design and synthesis of two triazoninecarbaldehyde derivatives using several chemical tools. Journal of Saudi Chemical Society Vol. 22, no. 2 (Feb. 2018), pp.183-197.
https://search.emarefa.net/detail/BIM-782277
نمط استشهاد الجمعية الطبية الأمريكية (AMA)
Figueroa Valverde, Lauro& Dıaz Cedillo, Francisco, Francisco& Garcıa Cervera, Elodia& Pool Gomez, Eduardo& Rosas Nexticapa, Marcela& Lopez Ramos, Marıa…[et al.]. Design and synthesis of two triazoninecarbaldehyde derivatives using several chemical tools. Journal of Saudi Chemical Society. 2018. Vol. 22, no. 2, pp.183-197.
https://search.emarefa.net/detail/BIM-782277
نوع البيانات
مقالات
لغة النص
الإنجليزية
الملاحظات
Includes bibliographical references : p. 196-197
رقم السجل
BIM-782277
قاعدة معامل التأثير والاستشهادات المرجعية العربي "ارسيف Arcif"
أضخم قاعدة بيانات عربية للاستشهادات المرجعية للمجلات العلمية المحكمة الصادرة في العالم العربي
تقوم هذه الخدمة بالتحقق من التشابه أو الانتحال في الأبحاث والمقالات العلمية والأطروحات الجامعية والكتب والأبحاث باللغة العربية، وتحديد درجة التشابه أو أصالة الأعمال البحثية وحماية ملكيتها الفكرية. تعرف اكثر