Synthesis and studying of dendrimers functionalized with carbon disulfide derivatives
Other Title(s)
تحضير و دراسة مركبات متبلمرة متشعبة تحتوي في نهاياتها على ثنائي كبريتيد الكربون
Dissertant
Mubayyidin, Ahmad Abd al-Qadir
Thesis advisor
Comitee Members
Ali, Basim Faris
al-Salah, Hasan A.
al-Saduni, Haytham H.
University
Al albayt University
Faculty
Faculty of Sciences
Department
Department of Chemistry
University Country
Jordan
Degree
Master
Degree Date
2008
English Abstract
In this work divergent approach (from the central core out to the periphery) was used to synthesize dendrimers (Scheme).
The multi was readily prepared according to the reported method by the reaction of ethylenediamine with methylacrylate.
Dendrimer 1 was then converted to the hydrazide derivative (2) by the reaction with hydrazine hydrate.
The corresponding dithiocarbazetes derivative (3) was then prepared by the addition of carbon disulphide to the resulted hydrazide, which upon heating educes 3, 4-oxadiazole-2-thione (4 and 4").
Alkylation of the 1, 3, 4-oxadiazole-2-thione derivative using methyl iodide yielded the 1, 3, 4-oxadiazole-2-methylthione derivative (5-811).
The compounds were characterized by elemental analyses and some standard spectroscopic techniques such as 13C- nuclear magnetic resonance, mass spectroscopy and infrared spectroscopy.
Main Subjects
No. of Pages
106
Table of Contents
Table of contents.
Abstract.
Chapter One : introduction.
Chapter Two : experimental part.
Chapter Three : reasults and discussion.
References.
American Psychological Association (APA)
Mubayyidin, Ahmad Abd al-Qadir. (2008). Synthesis and studying of dendrimers functionalized with carbon disulfide derivatives. (Master's theses Theses and Dissertations Master). Al albayt University, Jordan
https://search.emarefa.net/detail/BIM-321430
Modern Language Association (MLA)
Mubayyidin, Ahmad Abd al-Qadir. Synthesis and studying of dendrimers functionalized with carbon disulfide derivatives. (Master's theses Theses and Dissertations Master). Al albayt University. (2008).
https://search.emarefa.net/detail/BIM-321430
American Medical Association (AMA)
Mubayyidin, Ahmad Abd al-Qadir. (2008). Synthesis and studying of dendrimers functionalized with carbon disulfide derivatives. (Master's theses Theses and Dissertations Master). Al albayt University, Jordan
https://search.emarefa.net/detail/BIM-321430
Language
English
Data Type
Arab Theses
Record ID
BIM-321430
